Features of cubic Ni3C and NiC carbides obtained by HT-HP sintering

O.I. Nakonechna; D.A. Stratiichuk; A.M. Kuryliuk; N.N. Belyavina

doi:10.15330/pcss.23.1.34-39

Authors

O.I. Nakonechna Taras Shevchenko National University of Kyiv
D.A. Stratiichuk V. Bakul Institute for Superhard Materials, NAS of Ukraine
A.M. Kuryliuk Taras Shevchenko National University of Kyiv
N.N. Belyavina Taras Shevchenko National University of Kyiv

DOI:

https://doi.org/10.15330/pcss.23.1.34-39

Keywords:

mechanical alloying, nanoscale material, x-ray diffraction, crystal structure, microhardness

Abstract

In this work NiC carbides were manufactured by HP-HT sintering of mechanically alloyed charges of the elemental Ni–carbon nanotubes (CNT) or Ni–Graphite. Structural features of the materials obtained were characterized by X-ray diffraction and scanning electron microscopy. X-ray diffraction studies have revealed that the crystal lattice of nickel carbide obtained from mechanically alloyed Ni–CNT charge is supplemented with additional Carbon atoms from the graphite shell of the high-pressure cell at HT-HP sintering. On the other hand, nickel carbide fabricated from mechanically alloyed Ni–Graphite charge retains its composition. It is shown that materials studied in this work demonstrate an advanced value of microhardness (up to 7 GPa).

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